TLC Fingerprinting and Pattern Recognition Methods in the Assessment of Authenticity of Poplar-Type Propolis.
Identifieur interne : 001649 ( Main/Exploration ); précédent : 001648; suivant : 001650TLC Fingerprinting and Pattern Recognition Methods in the Assessment of Authenticity of Poplar-Type Propolis.
Auteurs : Dušanka Milojkovi Opsenica [Serbie] ; Petar Ristivojevi [Serbie] ; Jelena Trifkovi [Serbie] ; Irena Vovk [Slovénie] ; Dražen Luši [Croatie] ; Živoslav Teši [Serbie]Source :
- Journal of chromatographic science [ 1945-239X ] ; 2016.
Descripteurs français
- KwdFr :
- Abeilles (physiologie), Analyse en composantes principales (MeSH), Animaux (MeSH), Chromatographie sur couche mince (normes), Cires (composition chimique), Croatie (MeSH), Flavonoïdes (isolement et purification), Humains (MeSH), Phénols (isolement et purification), Populus (MeSH), Propolis (composition chimique), Résines végétales (composition chimique), Serbie (MeSH), Slovénie (MeSH), Traitement d'image par ordinateur (statistiques et données numériques).
- MESH :
- composition chimique : Cires, Propolis, Résines végétales.
- isolement et purification : Flavonoïdes, Phénols.
- normes : Chromatographie sur couche mince.
- physiologie : Abeilles.
- statistiques et données numériques : Traitement d'image par ordinateur.
- Analyse en composantes principales, Animaux, Croatie, Humains, Populus, Serbie, Slovénie.
English descriptors
- KwdEn :
- Animals (MeSH), Bees (physiology), Chromatography, Thin Layer (standards), Croatia (MeSH), Flavonoids (isolation & purification), Humans (MeSH), Image Processing, Computer-Assisted (statistics & numerical data), Phenols (isolation & purification), Populus (MeSH), Principal Component Analysis (MeSH), Propolis (chemistry), Resins, Plant (chemistry), Serbia (MeSH), Slovenia (MeSH), Waxes (chemistry).
- MESH :
- chemical , chemistry : Propolis, Resins, Plant, Waxes.
- chemical , isolation & purification : Flavonoids, Phenols.
- physiology : Bees.
- standards : Chromatography, Thin Layer.
- statistics & numerical data : Image Processing, Computer-Assisted.
- Animals, Croatia, Humans, Populus, Principal Component Analysis, Serbia, Slovenia.
Abstract
Propolis is a "natural" remedy with prominent biological activity, which is used as dietary supplement. In the absence of clinical studies that would substantiate these claims, information on the biological activity of propolis is valuable. This study comprises chromatographic, image processing and chemometric approach for phenolic profiling of Serbian, Croatian and Slovenian propolis test solutions. Modern thin-layer chromatography equipment in combination with software for image processing was applied for fingerprinting and data acquisition, whereas the principal component analysis was used as pattern recognition method. Characterization of phenolic profile was performed along with the determination of the botanical and geographical origin of propolis. High-performance thin-layer chromatograms reveal that Central and Southeastern European propolis samples are rich in flavonoids. In addition, phenolic compounds proved to be suitable markers for the determination of European propolis authenticity.
DOI: 10.1093/chromsci/bmw024
PubMed: 26931733
Affiliations:
Links toward previous steps (curation, corpus...)
Le document en format XML
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Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia.</nlm:affiliation><country xml:lang="fr">Serbie</country><wicri:regionArea>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158</wicri:regionArea><wicri:noRegion>Belgrade 11158</wicri:noRegion></affiliation></author></titleStmt><publicationStmt><idno type="wicri:source">PubMed</idno><date when="2016">2016</date><idno type="RBID">pubmed:26931733</idno><idno type="pmid">26931733</idno><idno type="doi">10.1093/chromsci/bmw024</idno><idno type="wicri:Area/Main/Corpus">001889</idno><idno type="wicri:explorRef" wicri:stream="Main" wicri:step="Corpus" wicri:corpus="PubMed">001889</idno><idno type="wicri:Area/Main/Curation">001889</idno><idno type="wicri:explorRef" wicri:stream="Main" wicri:step="Curation">001889</idno><idno type="wicri:Area/Main/Exploration">001889</idno></publicationStmt><sourceDesc><biblStruct><analytic><title xml:lang="en">TLC Fingerprinting and Pattern Recognition Methods in the Assessment of Authenticity of Poplar-Type Propolis.</title><author><name sortKey="Milojkovi Opsenica, Dusanka" sort="Milojkovi Opsenica, Dusanka" uniqKey="Milojkovi Opsenica D" first="Dušanka" last="Milojkovi Opsenica">Dušanka Milojkovi Opsenica</name><affiliation wicri:level="1"><nlm:affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia dusankam@chem.bg.ac.rs.</nlm:affiliation><country wicri:rule="url">Serbie</country><wicri:regionArea>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158</wicri:regionArea><wicri:noRegion>Belgrade 11158</wicri:noRegion></affiliation></author><author><name sortKey="Ristivojevi, Petar" sort="Ristivojevi, Petar" uniqKey="Ristivojevi P" first="Petar" last="Ristivojevi">Petar Ristivojevi</name><affiliation wicri:level="1"><nlm:affiliation>Innovation Centre of Faculty of Chemistry Ltd, Studentski trg 12-16, Belgrade 11000, Serbia.</nlm:affiliation><country xml:lang="fr">Serbie</country><wicri:regionArea>Innovation Centre of Faculty of Chemistry Ltd, Studentski trg 12-16, Belgrade 11000</wicri:regionArea><wicri:noRegion>Belgrade 11000</wicri:noRegion></affiliation></author><author><name sortKey="Trifkovi, Jelena" sort="Trifkovi, Jelena" uniqKey="Trifkovi J" first="Jelena" last="Trifkovi">Jelena Trifkovi</name><affiliation wicri:level="1"><nlm:affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia.</nlm:affiliation><country xml:lang="fr">Serbie</country><wicri:regionArea>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158</wicri:regionArea><wicri:noRegion>Belgrade 11158</wicri:noRegion></affiliation></author><author><name sortKey="Vovk, Irena" sort="Vovk, Irena" uniqKey="Vovk I" first="Irena" last="Vovk">Irena Vovk</name><affiliation wicri:level="1"><nlm:affiliation>Laboratory for Food Chemistry, National Institute of Chemistry, Hajdrihova 19, Ljubljana SI-1000, Slovenia.</nlm:affiliation><country xml:lang="fr">Slovénie</country><wicri:regionArea>Laboratory for Food Chemistry, National Institute of Chemistry, Hajdrihova 19, Ljubljana SI-1000</wicri:regionArea><wicri:noRegion>Ljubljana SI-1000</wicri:noRegion></affiliation></author><author><name sortKey="Lusi, Drazen" sort="Lusi, Drazen" uniqKey="Lusi D" first="Dražen" last="Luši">Dražen Luši</name><affiliation wicri:level="1"><nlm:affiliation>Department of Environmental Health, Faculty of Medicine, University of Rijeka, Braće Branchetta 20, Rijeka HR-51000, Croatia.</nlm:affiliation><country xml:lang="fr">Croatie</country><wicri:regionArea>Department of Environmental Health, Faculty of Medicine, University of Rijeka, Braće Branchetta 20, Rijeka HR-51000</wicri:regionArea><wicri:noRegion>Rijeka HR-51000</wicri:noRegion></affiliation></author><author><name sortKey="Tesi, Zivoslav" sort="Tesi, Zivoslav" uniqKey="Tesi Z" first="Živoslav" last="Teši">Živoslav Teši</name><affiliation wicri:level="1"><nlm:affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia.</nlm:affiliation><country xml:lang="fr">Serbie</country><wicri:regionArea>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158</wicri:regionArea><wicri:noRegion>Belgrade 11158</wicri:noRegion></affiliation></author></analytic><series><title level="j">Journal of chromatographic science</title><idno type="eISSN">1945-239X</idno><imprint><date when="2016" type="published">2016</date></imprint></series></biblStruct></sourceDesc></fileDesc><profileDesc><textClass><keywords scheme="KwdEn" xml:lang="en"><term>Animals (MeSH)</term><term>Bees (physiology)</term><term>Chromatography, Thin Layer (standards)</term><term>Croatia (MeSH)</term><term>Flavonoids (isolation & purification)</term><term>Humans (MeSH)</term><term>Image Processing, Computer-Assisted (statistics & numerical data)</term><term>Phenols (isolation & purification)</term><term>Populus (MeSH)</term><term>Principal Component Analysis (MeSH)</term><term>Propolis (chemistry)</term><term>Resins, Plant (chemistry)</term><term>Serbia (MeSH)</term><term>Slovenia (MeSH)</term><term>Waxes (chemistry)</term></keywords><keywords scheme="KwdFr" xml:lang="fr"><term>Abeilles (physiologie)</term><term>Analyse en composantes principales (MeSH)</term><term>Animaux (MeSH)</term><term>Chromatographie sur couche mince (normes)</term><term>Cires (composition chimique)</term><term>Croatie (MeSH)</term><term>Flavonoïdes (isolement et purification)</term><term>Humains (MeSH)</term><term>Phénols (isolement et purification)</term><term>Populus (MeSH)</term><term>Propolis (composition chimique)</term><term>Résines végétales (composition chimique)</term><term>Serbie (MeSH)</term><term>Slovénie (MeSH)</term><term>Traitement d'image par ordinateur (statistiques et données numériques)</term></keywords><keywords scheme="MESH" type="chemical" qualifier="chemistry" xml:lang="en"><term>Propolis</term><term>Resins, Plant</term><term>Waxes</term></keywords><keywords scheme="MESH" type="chemical" qualifier="isolation & purification" xml:lang="en"><term>Flavonoids</term><term>Phenols</term></keywords><keywords scheme="MESH" qualifier="composition chimique" xml:lang="fr"><term>Cires</term><term>Propolis</term><term>Résines végétales</term></keywords><keywords scheme="MESH" qualifier="isolement et purification" xml:lang="fr"><term>Flavonoïdes</term><term>Phénols</term></keywords><keywords scheme="MESH" qualifier="normes" xml:lang="fr"><term>Chromatographie sur couche mince</term></keywords><keywords scheme="MESH" qualifier="physiologie" xml:lang="fr"><term>Abeilles</term></keywords><keywords scheme="MESH" qualifier="physiology" xml:lang="en"><term>Bees</term></keywords><keywords scheme="MESH" qualifier="standards" xml:lang="en"><term>Chromatography, Thin Layer</term></keywords><keywords scheme="MESH" qualifier="statistics & numerical data" xml:lang="en"><term>Image Processing, Computer-Assisted</term></keywords><keywords scheme="MESH" qualifier="statistiques et données numériques" xml:lang="fr"><term>Traitement d'image par ordinateur</term></keywords><keywords scheme="MESH" xml:lang="en"><term>Animals</term><term>Croatia</term><term>Humans</term><term>Populus</term><term>Principal Component Analysis</term><term>Serbia</term><term>Slovenia</term></keywords><keywords scheme="MESH" xml:lang="fr"><term>Analyse en composantes principales</term><term>Animaux</term><term>Croatie</term><term>Humains</term><term>Populus</term><term>Serbie</term><term>Slovénie</term></keywords></textClass></profileDesc></teiHeader><front><div type="abstract" xml:lang="en">Propolis is a "natural" remedy with prominent biological activity, which is used as dietary supplement. In the absence of clinical studies that would substantiate these claims, information on the biological activity of propolis is valuable. This study comprises chromatographic, image processing and chemometric approach for phenolic profiling of Serbian, Croatian and Slovenian propolis test solutions. Modern thin-layer chromatography equipment in combination with software for image processing was applied for fingerprinting and data acquisition, whereas the principal component analysis was used as pattern recognition method. Characterization of phenolic profile was performed along with the determination of the botanical and geographical origin of propolis. High-performance thin-layer chromatograms reveal that Central and Southeastern European propolis samples are rich in flavonoids. In addition, phenolic compounds proved to be suitable markers for the determination of European propolis authenticity. </div></front></TEI><pubmed><MedlineCitation Status="MEDLINE" Owner="NLM"><PMID Version="1">26931733</PMID><DateCompleted><Year>2018</Year><Month>02</Month><Day>05</Day></DateCompleted><DateRevised><Year>2018</Year><Month>10</Month><Day>25</Day></DateRevised><Article PubModel="Print-Electronic"><Journal><ISSN IssnType="Electronic">1945-239X</ISSN><JournalIssue CitedMedium="Internet"><Volume>54</Volume><Issue>7</Issue><PubDate><Year>2016</Year><Month>Aug</Month></PubDate></JournalIssue><Title>Journal of chromatographic science</Title><ISOAbbreviation>J Chromatogr Sci</ISOAbbreviation></Journal><ArticleTitle>TLC Fingerprinting and Pattern Recognition Methods in the Assessment of Authenticity of Poplar-Type Propolis.</ArticleTitle><Pagination><MedlinePgn>1077-83</MedlinePgn></Pagination><ELocationID EIdType="doi" ValidYN="Y">10.1093/chromsci/bmw024</ELocationID><Abstract><AbstractText>Propolis is a "natural" remedy with prominent biological activity, which is used as dietary supplement. In the absence of clinical studies that would substantiate these claims, information on the biological activity of propolis is valuable. This study comprises chromatographic, image processing and chemometric approach for phenolic profiling of Serbian, Croatian and Slovenian propolis test solutions. Modern thin-layer chromatography equipment in combination with software for image processing was applied for fingerprinting and data acquisition, whereas the principal component analysis was used as pattern recognition method. Characterization of phenolic profile was performed along with the determination of the botanical and geographical origin of propolis. High-performance thin-layer chromatograms reveal that Central and Southeastern European propolis samples are rich in flavonoids. In addition, phenolic compounds proved to be suitable markers for the determination of European propolis authenticity. </AbstractText><CopyrightInformation>© The Author 2016. Published by Oxford University Press. All rights reserved. For Permissions, please email: journals.permissions@oup.com.</CopyrightInformation></Abstract><AuthorList CompleteYN="Y"><Author ValidYN="Y"><LastName>Milojković Opsenica</LastName><ForeName>Dušanka</ForeName><Initials>D</Initials><AffiliationInfo><Affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia dusankam@chem.bg.ac.rs.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Ristivojević</LastName><ForeName>Petar</ForeName><Initials>P</Initials><AffiliationInfo><Affiliation>Innovation Centre of Faculty of Chemistry Ltd, Studentski trg 12-16, Belgrade 11000, Serbia.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Trifković</LastName><ForeName>Jelena</ForeName><Initials>J</Initials><AffiliationInfo><Affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Vovk</LastName><ForeName>Irena</ForeName><Initials>I</Initials><AffiliationInfo><Affiliation>Laboratory for Food Chemistry, National Institute of Chemistry, Hajdrihova 19, Ljubljana SI-1000, Slovenia.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Lušić</LastName><ForeName>Dražen</ForeName><Initials>D</Initials><AffiliationInfo><Affiliation>Department of Environmental Health, Faculty of Medicine, University of Rijeka, Braće Branchetta 20, Rijeka HR-51000, Croatia.</Affiliation></AffiliationInfo></Author><Author ValidYN="Y"><LastName>Tešić</LastName><ForeName>Živoslav</ForeName><Initials>Ž</Initials><AffiliationInfo><Affiliation>Chair of Analytical Chemistry and Centre of Excellence for Molecular Food Sciences, University of Belgrade - Faculty of Chemistry, PO Box 51, Belgrade 11158, Serbia.</Affiliation></AffiliationInfo></Author></AuthorList><Language>eng</Language><PublicationTypeList><PublicationType UI="D016428">Journal Article</PublicationType></PublicationTypeList><ArticleDate DateType="Electronic"><Year>2016</Year><Month>02</Month><Day>29</Day></ArticleDate></Article><MedlineJournalInfo><Country>United States</Country><MedlineTA>J Chromatogr Sci</MedlineTA><NlmUniqueID>0173225</NlmUniqueID><ISSNLinking>0021-9665</ISSNLinking></MedlineJournalInfo><ChemicalList><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D005419">Flavonoids</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D010636">Phenols</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D012116">Resins, Plant</NameOfSubstance></Chemical><Chemical><RegistryNumber>0</RegistryNumber><NameOfSubstance UI="D014885">Waxes</NameOfSubstance></Chemical><Chemical><RegistryNumber>2ZA36H0S2V</RegistryNumber><NameOfSubstance UI="C038228">beeswax</NameOfSubstance></Chemical><Chemical><RegistryNumber>9009-62-5</RegistryNumber><NameOfSubstance UI="D011429">Propolis</NameOfSubstance></Chemical></ChemicalList><CitationSubset>IM</CitationSubset><MeshHeadingList><MeshHeading><DescriptorName UI="D000818" MajorTopicYN="N">Animals</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D001516" MajorTopicYN="N">Bees</DescriptorName><QualifierName UI="Q000502" MajorTopicYN="N">physiology</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D002855" MajorTopicYN="N">Chromatography, Thin Layer</DescriptorName><QualifierName UI="Q000592" MajorTopicYN="Y">standards</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D017523" MajorTopicYN="N">Croatia</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D005419" MajorTopicYN="N">Flavonoids</DescriptorName><QualifierName UI="Q000302" MajorTopicYN="Y">isolation & purification</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D006801" MajorTopicYN="N">Humans</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D007091" MajorTopicYN="N">Image Processing, Computer-Assisted</DescriptorName><QualifierName UI="Q000706" MajorTopicYN="Y">statistics & numerical data</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D010636" MajorTopicYN="N">Phenols</DescriptorName><QualifierName UI="Q000302" MajorTopicYN="Y">isolation & purification</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D032107" MajorTopicYN="N">Populus</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D025341" MajorTopicYN="N">Principal Component Analysis</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D011429" MajorTopicYN="N">Propolis</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="Y">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D012116" MajorTopicYN="N">Resins, Plant</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading><MeshHeading><DescriptorName UI="D055771" MajorTopicYN="N">Serbia</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D017524" MajorTopicYN="N">Slovenia</DescriptorName></MeshHeading><MeshHeading><DescriptorName UI="D014885" MajorTopicYN="N">Waxes</DescriptorName><QualifierName UI="Q000737" MajorTopicYN="N">chemistry</QualifierName></MeshHeading></MeshHeadingList></MedlineCitation><PubmedData><History><PubMedPubDate PubStatus="received"><Year>2015</Year><Month>12</Month><Day>17</Day></PubMedPubDate><PubMedPubDate PubStatus="entrez"><Year>2016</Year><Month>3</Month><Day>3</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="pubmed"><Year>2016</Year><Month>3</Month><Day>5</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate><PubMedPubDate PubStatus="medline"><Year>2018</Year><Month>2</Month><Day>6</Day><Hour>6</Hour><Minute>0</Minute></PubMedPubDate></History><PublicationStatus>ppublish</PublicationStatus><ArticleIdList><ArticleId IdType="pubmed">26931733</ArticleId><ArticleId IdType="pii">bmw024</ArticleId><ArticleId IdType="doi">10.1093/chromsci/bmw024</ArticleId></ArticleIdList></PubmedData></pubmed><affiliations><list><country><li>Croatie</li><li>Serbie</li><li>Slovénie</li></country></list><tree><country name="Serbie"><noRegion><name sortKey="Milojkovi Opsenica, Dusanka" sort="Milojkovi Opsenica, Dusanka" uniqKey="Milojkovi Opsenica D" first="Dušanka" last="Milojkovi Opsenica">Dušanka Milojkovi Opsenica</name></noRegion><name sortKey="Ristivojevi, Petar" sort="Ristivojevi, Petar" uniqKey="Ristivojevi P" first="Petar" last="Ristivojevi">Petar Ristivojevi</name><name sortKey="Tesi, Zivoslav" sort="Tesi, Zivoslav" uniqKey="Tesi Z" first="Živoslav" last="Teši">Živoslav Teši</name><name sortKey="Trifkovi, Jelena" sort="Trifkovi, Jelena" uniqKey="Trifkovi J" first="Jelena" last="Trifkovi">Jelena Trifkovi</name></country><country name="Slovénie"><noRegion><name sortKey="Vovk, Irena" sort="Vovk, Irena" uniqKey="Vovk I" first="Irena" last="Vovk">Irena Vovk</name></noRegion></country><country name="Croatie"><noRegion><name sortKey="Lusi, Drazen" sort="Lusi, Drazen" uniqKey="Lusi D" first="Dražen" last="Luši">Dražen Luši</name></noRegion></country></tree></affiliations></record>Pour manipuler ce document sous Unix (Dilib)
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